By Richard W. Weiss
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Additional resources for Compounds of Germanium, Tin and Lead Including Biological Activity and Commercial Application: Covering the Literature from 1965 to 1968
Of Et2(MeCH:CHCH2)GeX with EtMgBr; X - C1, Br (467), in 79 and 82% yie1d, resp. (1798), X • I, in 85% yie1d (1798). By-prod. in rxn. of Et5GeH with (CH2:CH)2 in presence of cat. HePtC1 e at 100°, in 36% yie1d (1798). 9872 (1798), (far) IR spectrum (1798), GLC (467, 1798), cis-trans-ratio in product (467, 1798). Rxn. with: H + cat. Raney Ni ~ Et5GeBu (467, 1798). Br in EtBr ~ Et5GeBr + MeCH:CHCH2Br (467, 1798). HgBr2 ~ Et5GeBr + MeCH:CHCHeHgBr; kinetic data, inf1uence of solvent, rxn. mechanism (2715).
V) Deeo10rizes Br soln. (1221). (w) Rxn. with MePhSiH2 ~ (EtPhGeCH:CHSiMePhCH:CH)x (327). (x) IR speetrum (466, 1761). (y) NMR speetrum (1931). (z) Rxn. with CO 2 (CO)e ~ Ph2Ge[CiCRCo2 (CO)e]2 + CO; R = Pr, Ph (236A, 1222). (aa) Therma1 dee. CCH2 )x (2546).
CH2N2 ~ Ph2Ge(C:CHNHN:CH)2 (939). Ph2GeH2 ~ (CH:CHPh2GeCH:CH)x (327). : By rxn. of PhsGeBr with HC:CMgBr in EtzO in N atrn. (1438), in THF in 60% yie1d (2562). By rxn. , in 14% yie1d (939), in pyridine in good yie1d (1039). : m. ~ 147-60° (1438), IR (2562) and NMR (1026, 1474, 1931) spectra, GLC (2562), mo1. wt. (939), po1ymerizes in N atrn. at 150-200° (1438). Rxn. CH)2 ~ copo1ymer (1438). CSnPhs (1039)· Additiona1 tetraorganogerrnanes with acety1enic substituents are surnrnarized in Tab1e 8. IlE IIID I I IIID Synth.
Compounds of Germanium, Tin and Lead Including Biological Activity and Commercial Application: Covering the Literature from 1965 to 1968 by Richard W. Weiss